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应用生态学报 ›› 1991, Vol. 2 ›› Issue (2): 191-193.

• 研究论文 • 上一篇    

催化示波极谱法测定农作物中的微量铅

索有瑞1, 黄雅丽2   

  1. 1. 中国科学院西北高原生物研究所, 西宁 810001;
    2. 西宁市环境保护监测站, 西宁 810001
  • 收稿日期:1990-09-04 出版日期:1991-04-25 发布日期:1991-04-25

Catalytic wave oscillopolarographic determination of traces of lead in crops

Suo Yourui1, Huang Yali2   

  1. 1. Northwest Plateau Institute of Biology, Academia Sinica, Xining 810001;
    2. Environmental Monitoring Station of Xining, Xining 810001
  • Received:1990-09-04 Online:1991-04-25 Published:1991-04-25

Abstract: Asensitive polarographic catalytic wave system (Pb-0.24M HCl-0.6% NaAc-0.4% KI-0.4% ascorbic acid) for determining traces of lead in crops was proposed. The peak potential is-0.34V (vs. S. C. E.). The wave for the determination of lead within the range of 0—30μg/25ml is available. The detection limit of Pb is 0.002μg/ml. Eighteen metal ions and acid radicals are not interferential. The waves are clear and steady. The recovery is 92.6—107% and the variation coefficient is less than 3.41%.

Key words: Oscillopolarographic wave, Lead, Crops